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Aniline and water form an immiscible mixture. Which technique is most suitable for separating aniline from this mixture?
- Steam distillation
- Fractional distillation
- Simple distillation
- Distillation under reduced pressure
Correct answer: Steam distillation
Solution
Aniline (bp 184 deg C) is immiscible with water and would decompose near its boiling point. Steam distillation lets it co-distil with steam at about 98 deg C, well below its normal boiling point, without decomposition.
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